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Cryogenic grinding : ウィキペディア英語版 | Cryogenic grinding
Cryogenic grinding, also known as freezer milling, freezer grinding, and cryomilling, is the act of cooling or chilling a material and then reducing it into a small particle size. For example, thermoplastics are difficult to grind to small particle sizes at ambient temperatures because they soften, adhere in lumpy masses and clog screens. When chilled by dry ice, liquid carbon dioxide or liquid nitrogen, the thermoplastics can be finely ground to powders suitable for electrostatic spraying and other powder processes.〔http://composite.about.com/library/glossary/c/bldef-c1386.htm Cryogenic Grinding〕 Cryogenic grinding of plant and animal tissue is a technique used by microbiologists. Samples that require extraction of nucleic acids must be kept at −80 °C or lower during the entire extraction process. For samples that are soft or flexible at room temperature, cryogenic grinding may be the only viable technique for processing samples.〔()〕〔() 〕 A number of recent studies report on the processing and behavior of nanostructured materials via cryomilling.〔http://filer.funmat.no/FUNMAT_meeting_2006/FridayII_H2/9_deledda_0106.pdf〕 ==Freezer milling== Freezer milling is a type of cryogenic milling that uses a solenoid to mill samples. The solenoid moves the grinding media back and forth inside the vial, grinding the sample down to analytical fineness. This type of milling is especially useful in milling temperature sensitive samples, as samples are milled at liquid nitrogen temperatures. The idea behind using a solenoid is that the only "moving part" in the system is the grinding media inside the vial. The reason for this is that at liquid nitrogen temperatures (–196°C) any moving part will come under huge stress leading to potentially poor reliability. Cryogenic milling using a solenoid has been used for over 50 years and has been proved to be a very reliable method of processing temperature sensitive samples in the laboratory.
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